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Topic Review
Cellulose Nanocrystal (CNC) Gels: A Review
Cellulose nanocrystals (CNCs) are emerging nanomaterials derived from the most abundant renewable polymer on earth, being widely distributed in plants, bacteria, algae, etc., which can be extracted from these cellulosic sources through mechanical disintegration, controlled sulfuric acid hydrolysis and mixed acid hydrolysis.
  • 353
  • 18 Jul 2023
Topic Review
Applications of Metal-Organic Frameworks in Food Sample Preparation
Food samples such as milk, beverages, meat and chicken products, fish, etc. are complex and demanding matrices. Various novel materials such as molecular imprinted polymers (MIPs), carbon-based nanomaterials carbon nanotubes, graphene oxide and metal-organic frameworks (MOFs) have been recently introduced in sample preparation to improve clean up as well as to achieve better recoveries, all complying with green analytical chemistry demands. Metal-organic frameworks are hybrid organic inorganic materials, which have been used for gas storage, separation, catalysis and drug delivery. 
  • 312
  • 17 Jul 2023
Topic Review
Graphene Oxide for Organic Compounds Magnetic Solid-Phase Extraction
Graphene oxide (GO) is a chemical compound with a form similar to graphene that consists of one-atom-thick two-dimensional layers of sp2-bonded carbon. Graphene oxide exhibits high hydrophilicity and dispersibility. Thus, it is difficult to be separated from aqueous solutions. Therefore, functionalization with magnetic nanoparticles is performed in order to prepare a magnetic GO nanocomposite that combines the sufficient adsorption capacity of graphene oxide and the convenience of magnetic separation. Moreover, the magnetic material can be further functionalized with different groups to prevent aggregation and extends its potential application. A plethora of magnetic GO hybrid materials have been synthesized and successfully employed for the magnetic solid-phase extraction of organic compounds from environmental, agricultural, biological, and food samples. The developed GO nanocomposites exhibit satisfactory stability in aqueous solutions, as well as sufficient surface area.
  • 207
  • 17 Jul 2023
Topic Review
Microextraction Techniques with Deep Eutectic Solvents
The development and application of sustainable solvents has been a hot topic in different scientific and technological areas. Deep eutectic solvents (DESs), were introduced in 2001 as an alternative to ionic liquids (ILs). These showed a stronger ecofriendly profile, with easier and cheaper production, while having similar properties. DESs contain large, asymmetrical ions that have low lattice energy and, thus, low melting points. They are often acquired by the complexation of a quaternary ammonium salt with a metal salt or hydrogen bond donor (HBD).
  • 266
  • 17 Jul 2023
Topic Review
Applications of Fabric Phase Sorptive Extraction
Fabric phase sorptive extraction (FPSE) is a novel and green sample preparation technique introduced in 2014. FPSE utilizes a natural or synthetic permeable and flexible fabric substrate chemically coated with a sol-gel organic-inorganic hybrid sorbent in the form of ultra-thin coating, which leads to a fast and sensitive micro-extraction device. The flexible FPSE requires no modification of samples and allows direct extraction of analytes. Sol-gel sorbent-coated FPSE media possesses high chemical, solvent, and thermal stability due to the strong covalent bonding between the substrate and the sol-gel sorbent.
  • 224
  • 17 Jul 2023
Topic Review
Ionic Liquids in Miniaturized Microextraction Techniques
Green sample preparation is one of the most challenging aspects in green analytical chemistry. In this framework, miniaturized microextraction techniques have been developed and are widely performed due to their numerous positive features such as simplicity, limited need for organic solvents, instrumentation of low cost and short time of extraction. Some of the most important sample preparation techniques covered include solid-phase microextraction (SPME), dispersive liquid-liquid microextraction (DLLME), single-drop microextraction (SDME), stir bar sorptive extraction (SBSE), and stir cake sorptive extraction (SCSE).
  • 267
  • 17 Jul 2023
Topic Review
Sample Preparation Techniques Used in Food Analysis
Food samples are complex heterogenous matrices, where all analytes are distributed in a random manner. Food analysis involves sampling, homogenization, and sample preparation that increase the analytical accuracy and precision. Focusing on sample preparation it usually involves storage, particle size reduction, homogenization, weighting, dilution, filtration, extraction, clean-up, and derivatization. Proper sample preparation protocols result in matrix interference elimination and analyte preconcentration, thus affecting the selectivity, sensitivity, detection capability, and the overall performance of an analytical technique. The most time-consuming step in analytical method development is the optimization of the sample preparation protocol that includes analyte extraction and clean-up. Some of the most common sample preparation techniques used in food analysis are liquid-liquid extraction (LLE), solid-liquid extraction (SLE), solid-phase extraction (SPE), solid-phase microextraction (SPME), stir bar sorptive extraction (SBSE), supercritical fluid extraction (SFE), accelerated solvent extraction (ASE), ultrasonic, and Soxhlet extraction.
  • 1.0K
  • 17 Jul 2023
Topic Review
Molecularly Imprinted Polymers in Sample Preparation
Molecularly Imprinted Polymers (MIPs) are synthetic polymeric materials with imprinted sites complementary to a specific molecule and high affinity over analytes with analogous molecular structure. Extraction can benefit from the production of MIPs that can be applied as sorbents for the extraction of specific antibiotics. 
  • 448
  • 17 Jul 2023
Topic Review
Antibacterial Activities of 1,2,3-Triazolium Salts
1,2,3-Triazolium salts have demonstrated significant potential in the fields of medicine and agriculture, exhibiting exceptional antibacterial, antifungal, anticancer, and antileishmanial properties. Moreover, these salts can be utilized as additives or components to produce nano- and fiber-based materials with antibacterial properties. 
  • 363
  • 17 Jul 2023
Topic Review
Required Properties of the Corneal Endothelial Implants
Treating corneal diseases arising from injury to the corneal endothelium necessitates donor tissue, but these corneas are extremely scarce. As a result, researchers are dedicating significant efforts to exploring alternative approaches that do not rely on donor tissues. Among these, creating a tissue-engineered scaffold on which corneal endothelial cells can be transplanted holds particular fascination. Numerous functional materials, encompassing natural, semi-synthetic, and synthetic polymers, have already been studied in this regard.
  • 227
  • 17 Jul 2023
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