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Topic Review
Fabric Phase Sorptive Extraction in Sample Preparation
Fabric phase sorptive extraction (FPSE) is an evolutionary sample preparation approach which was introduced in 2014, meeting all green analytical chemistry (GAC) requirements by implementing a natural or synthetic permeable and flexible fabric substrate to host a chemically coated sol–gel organic–inorganic hybrid sorbent in the form of an ultra-thin coating. This construction results in a versatile, fast, and sensitive micro-extraction device. The user-friendly FPSE membrane allows direct extraction of analytes with no sample modification, thus eliminating/minimizing the sample pre-treatment steps, which are not only time consuming, but are also considered the primary source of major analyte loss. Sol–gel sorbent-coated FPSE membranes possess high chemical, solvent, and thermal stability due to the strong covalent bonding between the fabric substrate and the sol–gel sorbent coating. Subsequent to the extraction on FPSE membrane, a wide range of organic solvents can be used in a small volume to exhaustively back-extract the analytes after FPSE process, leading to a high preconcentration factor.
  • 264
  • 12 Jul 2023
Topic Review
Magnetic Sample Preparation Methods Prior to Liquid Chromatography
Magnetic nanomaterials and nanostructures compose an innovative subject in sample preparation. Most of them are designed according to the properties of the target analytes on each occasion. The unique characteristics of nanomaterials enhance the proficiency at extracting and enriching due to their selective adsorption ability as well as easy separation and surface modification. Their remarkable properties, such as superparamagnetism, biocompatibility and selectivity have established magnetic materials as very reliable options in sample preparation approaches.
  • 166
  • 12 Jul 2023
Topic Review
Crystal Structural Characterization Techniques in Degradation of Perovskite
The general chemical formula of halide perovskite materials is ABX3, where the A site can be occupied by organic cations, such as methyl ammonium (MA), formamidinium (FA), or inorganic cation cesium. The B site can be divalent cations, such as lead(Pb) or tin(Sn), while the X site consists of halide anions, such as chlorine(Cl), bromine(Br) or iodine(I). Due to the great variety of its chemical composition, halide perovskite forms a big material family with tunable optoelectronic properties.
  • 262
  • 12 Jul 2023
Topic Review
Iridium-Catalyzed Difunctionalization of Alkenes
Alkenes and their related analogs are a class of ideal starting materials for the construction of complex molecules, because they are readily available in bulk quantities from renewable resources and petrochemical feedstocks. They are also considered to be the most cost-effective and widely used raw material for organic synthesis, and due to the diversity of functional groups, they are used very frequently in different chemical industries. As basic functionalities, the exploration of efficient methods for the selective functionalization of alkenes has been a continuous pursuit throughout the history of organic chemistry.
  • 399
  • 12 Jul 2023
Topic Review
Decellularized Extracellular Matrix from Different Sources
The decellularized extracellular matrix (dECM) is capable of promoting stem cell proliferation, migration, adhesion, and differentiation. It is a promising biomaterial for application and clinical translation in the field of periodontal tissue engineering as it most effectively preserves the complex array of ECM components as they are in native tissue, providing ideal cues for regeneration and repair of damaged periodontal tissue. dECMs of different origins have different advantages and characteristics in promoting the regeneration of periodontal tissue. dECM can be used directly or dissolved in liquid for better flowability.
  • 306
  • 12 Jul 2023
Topic Review
The Chemical Fingerprint of Fortified Wines
The chemical fingerprint of fortified wines is very complex and fascinating, being constituted by several hundred volatile and non-volatile chemical groups, such as terpenoids, pyrazines, esters, alcohols, acids, furanic compounds, phenolic compounds, and organic acids, among others. These chemical groups were present in fortified wines at different volatilities, polarities, and concentration ranges, from a few ng/L to mg/L. However, the quality of wine also depends on several parameters, such as grape variety, vineyard location, terroir, and vinification conditions (e.g., fermentation, ageing), among others. 
  • 681
  • 12 Jul 2023
Topic Review
Phosphonium-Based Polyelectrolytes
Phosphorous is an essential element for the life of organisms, and phosphorus-based compounds have many uses in industry, such as flame retardancy reagents, ingredients in fertilizers, pyrotechnics, etc. Ionic liquids are salts with melting points lower than the boiling point of water. The term “polymerized ionic liquids” (PILs) refers to a class of polyelectrolytes that contain an ionic liquid (IL) species in each monomer repeating unit and are connected by a polymeric backbone to form macromolecular structures. PILs provide a new class of polymeric materials by combining some of the distinctive qualities of ILs in the polymer chain. Ionic liquids have been identified as attractive prospects for a variety of applications due to the high stability (thermal, chemical, and electrochemical) and high mobility of their ions, but their practical applicability is constrained because they lack the benefits of both liquids and solids, suffering from both leakage issues and excessive viscosity. PILs are garnering for developing non-volatile and non-flammable solid electrolytes.
  • 371
  • 12 Jul 2023
Topic Review
Pellet Production from Pruning and Alternative Forest Biomass
Typically, coniferous sawdust from debarked stems is used to make pellets. Given the high lignin content, which ensures strong binding and high calorific values, this feedstock provides the best quality available. However, finding alternative feedstocks for pellet production is crucial if small-scale pellet production is to be developed and used to support the economy and energy independence of rural communities. These communities have to be able to create pellets devoid of additives and without biomass pre-processing so that the feedstock price remains low. The features of pellets made from other sources of forest biomass, such as different types of waste, broadleaf species, and pruning biomass, have attracted some attention in this context.
  • 286
  • 12 Jul 2023
Topic Review
Structure, Spectral Properties and Chemistry of Spiropyrans
Spiropyrans (SP) are a well-studied class of photochromic compounds. These compounds are usually named in conformity with the IUPAC rules for nomenclature of heterocyclic spirocompounds, as derivatives of 1′,3′,3′-trimethyl-6-nitrospiro[2H-1-benzopyran-2,2′-indoline] or 1′,3′-dihydro-1′,3′,3′-trimethyl-6-nitrospiro[2H-1-benzopyran-2,2′-indole].
  • 1.1K
  • 11 Jul 2023
Topic Review
Classification of Bio-Magnetic Nanoparticles
Bio-magnetic nanoparticles (BMNPs) was introduced, describing a unique combination of physio-chemical properties of magnetic nanoparticles with their entirely biocompatible nature, which makes them particularly effective in various biomedical applications.
  • 276
  • 11 Jul 2023
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