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Topic Review
Plasmonic biosensing schemes for virus
The uncertain proportions of pandemic outbreaks have triggered the need of reliable and cost-effective protocols easily adaptable to the changing virulence of virus strains. In recent years, plasmonic biosensors are being increasingly applied for clinical diagnosis of viral and other infectious diseases. Typical plasmonic biosensing strategies rely on the versatility of SPR and LSPR as label-free detection systems capable of monitoring binding interactions in a short period of time. Nevertheless, the incorporation of technological advancements has precipitated the development of nanomaterial-based applications for improving the sensitivity and specificity of classical configurations. The unique optical properties of plasmonic nanostructures has been exploited in combination with SERS colorimetric, fluorescence or luminescence enhancement for viral diagnosis. Likewise, the development of plasmonic virus sensing approaches has also benefitted from the variety of virus biomarkers. Thus, a high number of virus plasmonic biosensors have prompted the advance of novel functionalization strategies to achieve the effective coverage of the biological receptor while ensuring the affinity and specificity towards the target viral nucleic acids, proteins or whole virus. The huge potential for single virus detection along with the effectiveness and simplicity of current plasmonic configurations will impact on the routine surveillance of virus in clinical settings during this decade.
  • 1.8K
  • 27 Oct 2020
Topic Review
Reductive Aminations with Metal Catalysts
Recently, N-substituted anilines have been the object of increasing research interest in the field of organic chemistry due to their role as key intermediates for the synthesis of important compounds such as polymers, dyes, drugs, agrochemicals and pharmaceutical products. Among the various methods reported in literature for the formation of C–N bonds to access secondary anilines, the one-pot reductive amination of aldehydes with nitroarenes is the most interesting procedure, because it allows to obtain diverse N-substituted aryl amines by simple reduction of nitro compounds followed by condensation with aldehydes and subsequent reduction of the imine intermediates. These kinds of tandem reactions are generally catalyzed by transition metal-based catalysts, mainly potentially reusable metal nanoparticles. 
  • 1.7K
  • 21 Apr 2021
Topic Review
Clean Ethanol from CO2 Reduction
Using renewable energy to convert CO2 to a clean fuel ethanol can not only reduce carbon emission by the utilization of CO2 as feedstock, but also store renewable energy as the widely used chemical and high-energy-density fuel, being considered as a perfect strategy to address current environment and energy issues. Developing efficient electrocatalysts, photocatalysts, and photoelectrocatalysts for CO2 reduction is the most crucial keystone for achieving this goal. Considerable progresses in CO2-based ethanol production have been made over the past decades. This review provides the general principles and summarizes the latest advancements of electrocatalytic, photocatalytic and photoelectrocatalytic CO2 conversion to ethanol. Furthermore, the main challenges and proposed future prospects are illustrated for further development of the clean fuel ethanol production.
  • 1.7K
  • 24 Nov 2020
Topic Review
Identification of New Psychoactive Substances
New (or novel) psychoactive substances (NPS) or “designer drugs”, substances that are not controlled by the 1961 Single Convention on Narcotic Drugs or the 1971 Convention on Psychotropic Substances, pose public health threats. NPS are widely available on the web, through local head shops, on streets and in schools. Many chemical and nucleic acid based methods can be used to detect and identify these substances.
  • 1.6K
  • 29 Oct 2020
Topic Review
Living Anionic Polymerization
Living anionic polymerization is a living polymerization technique involving an anionic propagating species. Living anionic polymerization was demonstrated by Szwarc and co workers in 1956. Their initial work was based on the polymerization of styrene and dienes. One of the remarkable features of living anionic polymerization is that the mechanism involves no formal termination step. In the absence of impurities, the carbanion would still be active and capable of adding another monomer. The chains will remain active indefinitely unless there is inadvertent or deliberate termination or chain transfer. This gave rise to two important consequences: The following experimental criteria have been proposed as a tool for identifying a system as living polymerization system. However, in practice, even in the absence of terminating agents, the concentration of the living anions will reduce with time due to a decay mechanism termed as spontaneous termination.
  • 1.6K
  • 31 Oct 2022
Topic Review
Pesticide residues detection by Characteristics
The excessive use or abuse of pesticides leads to residues in food, which can threaten human health. Therefore, there is an extremely urgent need for multi-analyte analysis techniques for the detection of pesticide residues, which can be applied as screening techniques for food safety monitoring and detection. Recent developments related to rapid multi-residue detection methods for pesticide residues are reviewed herein. Methods based on the inherent characteristics of pesticides are described in detail. Enzymatic inhibition-based sensors, near-infrared spectroscopy, and SERS spectroscopy based on the inherent characteristics are discussed.
  • 1.6K
  • 26 Aug 2020
Topic Review
Fluorescence Polarization-Based Bioassays
Fluorescence polarization holds considerable promise for bioanalytical systems because it allows the detection of selective interactions in real time and a choice of fluorophores, the detection of which the biosample matrix does not influence; thus, their choice simplifies and accelerates the preparation of samples. For decades, these possibilities were successfully applied in fluorescence polarization immunoassays based on differences in the polarization of fluorophore emissions excited by plane-polarized light, whether in a free state or as part of an immune complex. However, the results of recent studies demonstrate the efficacy of fluorescence polarization as a detected signal in many bioanalytical methods.
  • 1.6K
  • 17 Dec 2020
Topic Review
Neutralization
In chemistry, neutralization or neutralisation (see spelling differences) is a chemical reaction in which acid and a base react quantitatively with each other. In a reaction in water, neutralization results in there being no excess of hydrogen or hydroxide ions present in the solution. The pH of the neutralized solution depends on the acid strength of the reactants.
  • 1.6K
  • 22 Nov 2022
Topic Review
Determination of Steroids by High Performance Liquid Chromatography-Fluorescence
Steroids are compounds widely available in nature and synthesized for therapeutic and medical purposes. Although several analytical techniques are available for the quantification of steroids in clinical samples, their analysis is challenging due to their low levels and complex matrices. The efficiency and quick separation of the high performance liquid chromatography (HPLC) combined with the sensitivity, selectivity, simplicity, and cost-efficiency of fluorescence, make HPLC coupled to fluorescence detection (HPLC-FLD) an ideal tool for routine measurement and detection of steroids for clinical and medical applications.
  • 1.6K
  • 11 Apr 2022
Topic Review
Mass Spectrometry in Determination of Pesticide Residues
The extensive use of pesticides represents a risk to human health. Consequently, legal frameworks have been established to ensure food safety, including control programs for pesticide residues. In this context, the performance of analytical methods acquires special relevance. Such methods are expected to be able to determine the largest number of compounds at trace concentration levels in complex food matrices, which represents a great analytical challenge. Technical advances in mass spectrometry (MS) have led to the development of more efficient analytical methods for the determination of pesticides. 
  • 1.5K
  • 15 Jun 2022
Topic Review
Near-Infrared Spectrum of Olive Oils
Olive oil is regarded as one of the healthiest food oils due to its high content in triglycerides with unsaturated acids, mainly oleic acid, and its phenolic composition. The analysis of the physico-chemical parameters of quality of olive oil is still carried out in laboratories using chemicals and generating waste, which is relatively costly and time-consuming. Among the various alternatives for the online or on-site measurement of these parameters, the available literature highlights the use of near-infrared spectroscopy (NIRS). 
  • 1.5K
  • 18 Apr 2022
Topic Review Peer Reviewed
Enantiomers and Their Resolution
Enantiomers share the same chemical formula but have different chemical structures, i.e., type of isomers. Enantiomers are present in several drugs, perfumes, food, and are a fundamental part of biomolecules. This subject is highly important for pharmaceutical companies. Enantiomeric drugs present different actuation in the human body; depending on the compound, one might combat the symptom, whereas its pair might cause damage. The separation of pairs of enantiomers requires a chiral environment that provokes a structural imbalance that conventional methods cannot provide. Enantioresolution is one of the most promissory studies that benefit several areas, such as pharmaceutical, biotechnology, food industry, and fine chemistry. Its resolution is of great importance, therefore, its main mechanisms of resolution will be explained herein.
  • 1.5K
  • 14 Apr 2022
Topic Review
Seaweed Phenolics
Seaweed, also referred to as macroalgae, have been studied as potential aquafeed ingredients since the late 1970s but have been implemented as a poultry feed supplement since the 1950s. Seaweed phenolics provide alternative ingredients that are complementary to synthetic additives used in aquaculture, possessing a broad spectrum of bioactive properties such as antimicrobial, antiviral, antifungal, anti-stress, antioxidant, anti-inflammatory, immunostimulant, and appetite stimulation. Also, their antioxidant properties retard lipid oxidation and preserve feed quality improving shelf life. 
  • 1.5K
  • 19 Jul 2022
Topic Review
MOFs for Mercury Detection
The advantages of metal organic frameworks (MOFs) are: existence of porosity to adsorb specific analyte, improved aqueous solubility, exceptional photophysical and chemical properties. MOFs are noted as exceptional candidates towards the detection and removal of specific analytes, particular for the detection/removal of environmental contaminants, such as heavy metal ions, toxic anions, hazardous gases, explosives, etc. Among heavy metal ions, mercury has been noted as a global hazard because of its high toxicity in the elemental (Hg0), divalent cationic (Hg2+), and methyl mercury (CH3Hg+) forms. To secure the environment and living organisms, many countries have imposed stringent regulations to monitor mercury at all costs. Regarding the detection/removal requirements of mercury, researchers have proposed and reported all kinds of MOFs-based luminescent/non-luminescent probes towards mercury.This review provides valuable information about the MOFs which have been engaged in detection and removal of elemental mercury and Hg2+ ions. Moreover, the involved mechanisms or adsorption isotherms related to sensors or removal studies are clarified for the readers. Finally, advantages and limitations of MOFs in mercury detection/removal are described together with future scopes.
  • 1.4K
  • 01 Jul 2021
Topic Review
Chemistry and Occurrence of Tropane Alkaloids in Foods
Tropane alkaloids (TAs) are natural toxins produced by different plants, mainly from the Solanaceae family. 
  • 1.4K
  • 08 Feb 2022
Topic Review
Approaches for Water Pollution Monitoring
Researchers are continuously rallying to enhance the detection of causal source for water pollution through either conventional or mostly advanced approaches focusing on spectrometry, high-throughput sequencing, and flow cytometry technology among others. From this review’s perspective, each pollution evaluation technology has its own advantages and it would be beneficial for several aspects of pollutants assessments to be combined and established as a complementary package for a better aquatic environmental management in the long run.
  • 1.4K
  • 15 Dec 2020
Topic Review
Discriminating between Parallel, Anti-Parallel and Hybrid G-Quadruplexes
G-quadruplexes (G4) are now extensively recognised as a peculiar non-canonical DNA geometry that plays a prime importance role in processes of biological relevance whose number is increasing continuously. The same is true for the less-studied RNA G4 counterpart. G4s are stable structures; their geometrical parameters may be finely tuned not only by the presence of particular sequences of nucleotides but also by the salt content of the medium or by a small molecule that may act as a peculiar topology inducer. 
  • 1.3K
  • 14 Jul 2022
Topic Review
Sample Preparation Techniques Used in Food Analysis
Food samples are complex heterogenous matrices, where all analytes are distributed in a random manner. Food analysis involves sampling, homogenization, and sample preparation that increase the analytical accuracy and precision. Focusing on sample preparation it usually involves storage, particle size reduction, homogenization, weighting, dilution, filtration, extraction, clean-up, and derivatization. Proper sample preparation protocols result in matrix interference elimination and analyte preconcentration, thus affecting the selectivity, sensitivity, detection capability, and the overall performance of an analytical technique. The most time-consuming step in analytical method development is the optimization of the sample preparation protocol that includes analyte extraction and clean-up. Some of the most common sample preparation techniques used in food analysis are liquid-liquid extraction (LLE), solid-liquid extraction (SLE), solid-phase extraction (SPE), solid-phase microextraction (SPME), stir bar sorptive extraction (SBSE), supercritical fluid extraction (SFE), accelerated solvent extraction (ASE), ultrasonic, and Soxhlet extraction.
  • 1.3K
  • 17 Jul 2023
Topic Review
Chenopodium album
Bathua (Chenopodium album) is a rich source of extensive-ranging nutrients, including bio-active carbohydrates, flavonoids and phenolics, minerals, and vitamins that translate to countless health benefits such as anticancer, antidiabetic, anti-inflammatory, antimicrobial, and antioxidant activity. Ascaridole, an important phytoconstituent present in aerial parts of the plant, contributes to its anthelmintic property. 
  • 1.3K
  • 05 Jul 2023
Topic Review
Photocatalysis for Air Purification
Photocatalysis since a long time has been recognized  as a eco-technology to fight air pollution. It is focused  on the generation of reactive oxygen species (ROSs) under light on the surface of a photocatalytic material. It could be applied in different manners such as for the purification of industrial polluted air, photoconversion of toxic gas into valuable products, self-cleaning systems, photocatalytic filters, etc. However, it faces some technological issues limiting its wide application in real-world.  
  • 1.3K
  • 17 May 2021
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