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Topic Review
Electronic Circular Dichroism
This entry provides an introduction to the basic concepts of Electronic Circular Dichroism (ECD) spectroscopy. It describes the fundamental principles, instrumentation, and different approaches for interpreting and predicting ECD spectra. It surveys the most popular modern applications of ECD for the structural analysis of organic compounds.
  • 21.2K
  • 24 May 2022
Topic Review
Methanol Mitigation during Fruit-Spirits Manufacturing
Methanol is a natural ingredient with major occurrence in fruit spirits, such as apple, pear, plum or cherry spirits, but also in spirits made from coffee pulp. The compound is formed during fermentation and the following mash storage by enzymatic hydrolysis of naturally present pectins. Methanol is toxic above certain threshold levels and legal limits have been set in most jurisdictions. Therefore, the methanol content needs to be mitigated and its level must be controlled. This article will review the several factors that influence the methanol content including the pH value of the mash, the addition of various yeast and enzyme preparations, fermentation temperature, mash storage, and most importantly the raw material quality and hygiene
  • 7.2K
  • 10 May 2021
Topic Review
MOFs and COFs
Metal-organic frameworks (MOFs) and covalent organic frameworks (COFs) are two innovative classes of porous coordination polymers. MOFs are three-dimensional materials made up of secondary building blocks comprised of metal ions/clusters and organic ligands whereas COFs are 2D or 3D highly porous organic solids made up by light elements (i.e., H, B, C, N, O). Both MOFs and COFs, being highly conjugated scaffolds, are very promising as photoactive materials for applications in photocatalysis and artificial photosynthesis because of their tunable electronic properties, high surface area, remarkable light and thermal stability, easy and relative low-cost synthesis, and structural versatility. 
  • 5.0K
  • 08 Dec 2020
Topic Review
Ascorbic Acid-Mediated Reactions
Ascorbic acid is a vitamin found in different types of food. It has tremendous medical applications in several different fields such as in pharmaceuticals, cosmetics, and in organic synthesis. 
  • 4.1K
  • 25 Nov 2020
Topic Review
Classical Nucleation Theory
Crystal nucleation determining the formation and assembly pathway of first organic materials is the central science of various scientific disciplines such as chemical, geochemical, biological, and synthetic materials. Classical nucleation theory (CNT)  applies to systems of small organic molecules with an emphasis on the molecular interpretation of nucleation kinetics. CNT holds that density fluctuations are concomitant with the development of crystalline order. In other words, a crystal nucleus has an identical structure to its bulk crystal. 
  • 3.4K
  • 22 Jul 2022
Topic Review
Metabolic N-Dealkylation and N-Oxidation
Metabolic reactions that occur at alkylamino moieties may provide insight into the roles of these moieties when they are parts of drug molecules that act at different receptors. N-dealkylation of N,N-dialkylamino moieties has been associated with retaining, attenuation or loss of pharmacologic activities of metabolites compared to their parent drugs. Further, N-dealkylation has resulted in clinically used drugs, activation of prodrugs, change of receptor selectivity, and providing potential for developing fully-fledged drugs.
  • 3.1K
  • 13 Apr 2021
Topic Review
Synthesis of Fragrances via Cycloaddition or Formal Cycloaddition
Fragrances, short for fragrance ingredients, is a type of compounds with a sweet smell or pleasant odor that has wide applications in the fine chemical industry, especially in perfumes, cosmetics, detergents and food additives. Since the discovery of the Diels–Alder reaction, the cycloaddition of π reactants serves as one of the most powerful methods for the construction of carbocycles, which has a broad application in the fragrance industry.
  • 3.0K
  • 21 Jun 2022
Topic Review
Covalent Adaptable Networks
Thermosets are known to be very reliable polymeric materials for high-performance and light-weight applications, due to their retained dimensional stability, chemical inertia and rigidity over a broad range of temperatures. However, once fully cured, they cannot be easily reshaped or reprocessed, thus leaving still unsolved the issues of recycling and the lack of technological flexibility. Vitrimers, introduced by Leibler et al. in 2011, are a valiant step in the direction of bridging the chasm between thermoplastics and thermosets. Owing to their dynamic covalent networks, they can retain mechanical stability and solvent resistance, but can also flow on demand upon heating. More generally, the family of Covalent Adaptable Networks (CANs) is gleaming with astounding potential, thanks to the huge variety of chemistries that may enable bond exchange. Arising from this signature feature, intriguing properties such as self-healing, recyclability and weldability may expand the horizons for thermosets in terms of improved life-span, sustainability and overall enhanced functionality and versatility. In this review, we present a comprehensive overview of the most promising studies featuring CANs and vitrimers specifically, with particular regard for their industrial applications. Investigations into composites and sustainable vitrimers from epoxy-based and elastomeric networks are covered in detail.
  • 3.0K
  • 26 Oct 2020
Topic Review
Natural Phenols
Phenols are widespread in nature, being the major components of several plants and essential oils. Natural phenols’ anti-microbial, anti-bacterial, anti-oxidant, pharmacological and nutritional properties are, nowadays, well established. Hence, given their peculiar biological role, numerous studies are currently ongoing to overcome their limitations, as well as to enhance their activity.
  • 2.9K
  • 29 Sep 2021
Topic Review
Chemical looping
Chemical looping technology in general, is the rising star in chemical technologies, which is capable of low CO2 emissions with applications in the production of heat, fuels, chemicals, and electricity. This entry discusses the technology in general, gives an overview of some pilot scale plants and the different chemical looping processes with focus on the production of heat and chemicals, highlights the importance of the development of oxygen carrier materials with suitable properties, 2.11.0.0 2.11.0.0
  • 2.9K
  • 02 Nov 2020
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